AN INTEGRATED APPROACH TO THE RESEARCH OF FIRE EXTINGUISHING POWDER AGENTS DURING FIRES EXAMINATION
Abstract and keywords
Abstract (English):
The article discusses the possibility of using a set of instrumental methods, such as morphological analysis, elemental analysis, X-ray phase analysis, infrared spectroscopy, ion chromatography or capillary electrophoresis to study the chemical composition of fire extinguishing powders during fire-technical examinations. Examples of the use of these methods in the investigation of real fires are given. It is described in detail how studies of fire extinguishing agents are carried out to answer questions related to establishing their composition, as well as identifying the compliance of the fire extinguishing powder submitted for study with technical documentation. It is shown that in order to obtain complete information about the chemical composition of the fire extinguishing agent, it is necessary to use a set of methods, since each of the considered methods provides additional information during the study.

Keywords:
fire extinguishing powder agents, fire extinguishing compositions, elemental analysis, morphological analysis, infrared spectroscopy, X-ray fluorescence analysis, X-ray phase analysis, scanning electron microscopy, infrared spectroscopy, fire-technical examination
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References

1. Fischer G., Leonard J.T. Effectiveness of Fire Extinguishing Powders Based on Small Scale Suppression Test. Washington. 1995. P. 24.

2. Baratov A.N., Vogman L.P. Ognetushaschie poroshkovye sostavy. M.: Stroyizdat, 1982. 72 s.

3. Nadubov V.A., Baratov A.N., Vogman L.P. Ognetushaschie poroshki. M.: VNIIPO MChS Rossii, 2014. 274 s.

4. Sabinin O.Yu., Agalarova S.M. Ognetushaschie poroshki. Problemy. Sostoyanie voprosa // Pozharovzryvobezopasnost'. 2007. T. 16. № 6. S. 63–68.

5. Udilov T.V. Issledovanie ognetushaschih poroshkovyh sostavov pri proizvodstve pozharno-tehnicheskoy ekspertizy // Deyatel'nost' pravoohranitel'nyh organov v sovremennyh usloviya: XXI Mezhdunar. nauch.-prakt. konf. Irkutsk: Vostochno-Sibirskiy in-t MVD Rossii, 2016. S. 44–46.

6. Identifikaciya komponentov ognetushaschih poroshkov metodom IK-spektroskopii / T.V. Frolova [i dr.] // Sovremennye problemy grazhdanskoy zaschity. 2021. № 2 (39). S. 102–107.

7. Ivanenko O.S. O vozmozhnosti primeneniya metodov termicheskogo analiza k ognetushaschim poroshkovym sostavam na osnove neorganicheskih veschestv // Pozharnaya i avariynaya bezopasnost': XV Mezhdunar. nauch.-prakt. konf. Ivanovo: Ivanovskaya pozh.-spas. akad. GPS MChS Rossii. 2020. S. 326–329.

8. Evaluation of the phase composition of (NH4)2SO4+(NH4)H2PO4 mixtures by X-ray diffractometry / L. Angel [et al.] // Journal of Alloys and Compounds. Vol. 475. Is. 1–2. P. 686–692.

9. Gorelik S.S., Skakov Yu.A., Rastorguev L.N. Rentgenograficheskiy i elektronno-opticheskiy analiz: ucheb. posobie dlya vuzov. M.: MISIS, 2002. 360 s.

10. Kross A. Vvedenie v prakticheskuyu infrakrasnuyu spektroskopiyu. M.: Izd-vo inostrannoy lit., 1961. 110 s.

11. Plyusnina I.I. Infrakrasnye spektry mineralov. M.: Izd-vo Moskovskogo un-ta, 1976, 175 s.

12. IK-spektroskopiya v neorganicheskoy tehnologii / R.Yu. Zinyuk [i dr.]. L.: Himiya, 1983. 160 s.

13. Fischer G., Leonard J.T. Effectiveness of Fire Extinguishing Powders Based on Small Scale Suppression Test. Washington. 1995. P. 24.

14. Baratov A.N., Vogman L.P. Fire extinguishing powder compositions. M.: Stroyizdat, 1982. 72 p.

15. Nadubov V.A., Baratov A.N., Vogman L.P. Fire extinguishing powders. M.: VNIIPO of EMERCOM of Russia, 2014. 274 p.

16. Sabinin O.Yu., Agalarova S.M. Fire extinguishing powders. Problems. State of the issue // Fire and explosion safety. 2007. T. 16. № 6. P. 63–68.

17. Udilov T.V. Study of fire extinguishing powder compositions in the production of fire-technical examination // Activities of law enforcement agencies in modern conditions: XXI International. scientific-practical conf. Irkutsk: East Siberian Institute of the Ministry of Internal Affairs of Russia, 2016. P. 44–46.

18. Identification of components of fire extinguishing powders using IR spectroscopy / T.V. Frolova [et al.] // Modern problems of civil protection. 2021. № 2 (39). P. 102–107.

19. Ivanenko O.S. On the possibility of using thermal analysis methods to fire extinguishing powder compositions based on inorganic substances // Pozharnaya and emergency safety: XV International. scientific-practical conf. Ivanovo: Ivanovo Fire Rescue. acad. State fire service of EMERCOM of Russia. 2020. P. 326–329.

20. Evaluation of the phase composition of (NH4)2SO4+(NH4)H2PO4 mixtures by X-ray diffractometry / L. Angel [et al.] // Journal of Alloys and Compounds. Vol. 475. Iss. 1–2. P. 686–692.

21. Gorelik S.S., Skakov Yu.A., Rastorguev L.N. X-ray and electron-optical analysis: textbook. manual for universities. M.: MISIS, 2002. 360 p.

22. Cross A. Introduction to practical infrared spectroscopy. M.: Foreign literary publishing house, 1961. 110 p.

23. Plyusnina I.I. Infrared spectra of minerals. M.: Publishing house Mosk. univ., 1976, 175 p.

24. IR spectroscopy in inorganic technology / R.Yu. Zinyuk [et al.]. L.: Chemistry, 1983. 160 p.

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